大賽璐手性固定相的新進(jìn)展(編輯修改稿)
2025-05-30 13:43 本頁面
【文章內(nèi)容簡介】 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes Sulindac Hydroxyzine 0 2 4 6 8 10 12 14 Minutes 0 5 10 15 20 25 30 Minutes NNClOOHO HOSOFIA IB IC ID nHex/IPA/DEA=80/20/, , 254nm, 25 oC nHex/IPA/TFA=60/40/, , 254nm, 25 oC 25cmL Part3：鍵合型固定相 IA 的互補(bǔ)性 IA IB IC ID nHex/EtOH=80/20, , 220nm, 25 oC nHex/IPA/DEA=95/5/, , 254nm, 25 oC 25cmL 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 2 4 6 8 10 12 14 Minutes 0 2 4 6 8 10 12 14 Minutes 0 2 4 6 8 10 12 14 Minutes 0 2 4 6 8 10 12 14 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes OONNClγPhenylγ butyrolactone Meclizine Part3：鍵合型固定相 IB 的互補(bǔ)性 IA IB IC ID 25cmL nHex/EtOH/DEA=50/50/, , 254nm, 25 oC nHex/IPA=98/2, , 220nm, 25 oC 0 2 4 6 8 10 12 14 Minutes 0 2 4 6 8 10 12 14 Minutes 0 2 4 6 8 10 12 14 Minutes 0 4 8 12 16 20 Minutes 0 4 8 12 16 20 Minutes 0 4 8 12 16 20 Minutes 0 4 8 12 16 20 Minutes 0 2 4 6 8 10 12 14 Minutes 1Phenylethyl alchol NHClS N H2OON OOHIndapamide Part3：鍵合型固定相 IC 的互補(bǔ)性 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 5Benzylhydantoin Chlorprenaline NHNHOOnHex/IPA=80/20, , 220nm, 25 oC nHex/IPA/DEA=98/2/, , 254nm, 25 oC 0 2 4 6 8 10 12 14 Minutes 0 2 4 6 8 10 12 14 Minutes 0 2 4 6 8 10 12 14 Minutes 0 2 4 6 8 10 12 14 Minutes NHO HClIA IB IC ID 25cmL Part3：鍵合型固定相 分離介紹 ? ID和 IA IB IC 有一定的互補(bǔ)性 ? 非傳統(tǒng)流動(dòng)相的使用示例 ? ID柱特別適用分離的化合物類型 ? 其他化合物分離示例 Part3：鍵合型固定相 Thioridazine 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes ADH ODH ASH OJH nHex/IPA/DEA =98/2/ nHex/EtOH/DEA =100/1/ 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes ID IC IB IA nHex/IPA/DEA =98/2/ nHex/EtOH/DEA =100/1/ SNNS25cmL. , 254nm, 25℃ nHex/CH2Cl2/EtOH/DEA =95/5/1/ ID 0 2 4 6 8 10 14 18 12 16 20 Minutes 0 2 4 6 8 10 14 18 12 16 20 Minutes nHex/MTBE/EtOH/DEA =95/5/1/ 完全分離 Part3：鍵合型固定相 Sulpiride 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes 0 5 10 15 20 25 30 Minutes
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