【正文】 adding 1gOP10 and twelve sodium dodecyl sulfate at 150 rpm, each monomer film performance is the synthesis of the best. Keywords: Acrylate, emulsion polymerization, terminated isocyana 攀枝花學(xué)院本科畢業(yè)設(shè)計（論文） 目錄 i 目 錄 1 緒論 ..................................................................................................................... 1 引言 ............................................................................................................. 1 丙烯酸樹脂涂料 ........................................................................................... 1 丙烯酸樹脂涂料的簡介 ....................................................................... 1 丙烯酸酯的分類 .................................................................................. 1 聚氨酯涂料 ................................................................................................... 3 聚氨酯涂料的簡介 .............................................................................. 3 雙組份聚氨酯涂料 .............................................................................. 3 單組份聚氨酯涂料 .............................................................................. 4 紫外光固化涂料 ........................................................................................... 4 紫外光固化原理 .................................................................................. 4 紫外光固化的設(shè)備 .............................................................................. 5 涂料合成方法 ............................................................................................... 6 乳液聚合 ............................................................................................ 6 原位聚合 ............................................................................................ 7 懸浮聚合 ............................................................................................ 7 接枝聚合 ............................................................................................ 8 本體聚合 ............................................................................................ 8 溶液聚合 ............................................................................................ 8 實驗方案及意義 ........................................................................................... 9 實驗方案 ................................................................................................ 9 實驗意義 ............................................................................................ 9 2 實驗部分 ............................................................................................................. 1 實驗儀器及藥品 ........................................................................................... 1 實驗儀器 ............................................................................................ 1 實驗藥品 ............................................................................................ 1 實驗配方 ...................................................................................................... 1 實驗步驟 ..................................................................................................... 2 丙烯酸酯樹脂的實驗步驟 .................................................................... 2 亞硫酸氫鈉封端 MDI 的實驗步驟 ........................................................ 3 實驗測試 ...................................................................................................... 3 產(chǎn)品外觀 ............................................................................................ 3 攀枝花學(xué)院本科畢業(yè)設(shè)計（論文） 目錄 ii 固含量 ............................................................................................... 4 轉(zhuǎn)化率 ................................................................................................ 4 粘度測試 ............................................................................................ 5 耐水性測試 ......................................................................................... 5 紅外光譜測試 ..................................................................................... 5 熱性能測試 ......................................................................................... 5 黏度的測試 ......................................................................................... 5 玻璃轉(zhuǎn)化溫度的計算 ........................................................................... 5 3 結(jié)果與討論 ........................................................................................................ 7 測試結(jié)果 ...................................................................................................... 7 實驗現(xiàn)象 ...................................................................................................... 8 實驗條件控制 ............................................................................................... 9 紅外光譜分析 ............................................................................................... 9 DSC 測試 ................................................................................................... 11 單體配比的影響 ......................................................................................... 11 4 結(jié)論 .................................................................................................................. 14 參考文獻 ...........