化學(xué)專業(yè)畢業(yè)論文鹵代芳烴轉(zhuǎn)化為酚的合成研究-資料下載頁
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【正文】 反應(yīng)方面的研究能夠更加繁榮。致 謝本論文是在XXX博士和XXX教授的悉心指導(dǎo)下完成的。許老師和馮老師對待工作勤奮敬業(yè)、待人處事寬容謙和、培養(yǎng)學(xué)生嚴(yán)禁不茍的精神給我留下了深刻印象，并潛移默化地影響著我的一生。他在科研上的創(chuàng)新意識和開放思維，使我在本課題的研究工作受益匪淺。在此，謹(jǐn)向他表示崇高的敬意和衷心的感謝！其次要感謝XXX學(xué)長、XXX學(xué)長、XX學(xué)姐、XX學(xué)長、XX學(xué)長、XX學(xué)長以及707的其他各位師兄師姐，他們在課題的研究中給予了我許多的意見和幫助，提出了許多開創(chuàng)性的想法，同時還傳授了我許多實驗的經(jīng)驗和操作方法，使我對縱向課題的研究有了較為深入的了解。同時還要感謝XXX、XX、XX等同學(xué)，他們在實驗過程中也給予了我很多的幫助。最后，謹(jǐn)以此文獻給我的父母，他們是我多年求學(xué)的動力，給予了我最無私的支持、理解和鼓勵。參考文獻[1](a)Prim,D。Campagne,.。Joseph,D.。Andrioletti,58,2041.(b)Ley,.。Thomas,42,5400.[2]Ullmann,34,2174.[3]Ullmann,36,2382.[4]Hartwig J metal catalyzed synthesis of arylamines and aryl ethers from aryl halides and triflates:scope and Chem,Int Ed,1998, 37(15):20462067.[5]Kunz K,Scholz U,Ganzer D. Renaissance of Ullmann and Goldberg reactionsprogress in copper catalyzed CN,CO and CS coupling. Synlett, 2003, (15):24282439.[6] Olivera R, SanMartin R,Dominguez novel palladiumeatalyzed inlramolecular diaryl ether formation．Tetrahedron Lett,2000, 41(22)：43574360．[7] Mann G, Hartwig J F,Nickelvs palladiumcatalyzed synthesis of protected phenols from aryl halides．J Org Chem,1997,62(16)：54135418．[8] Kuwabe Si，Torraca K E, Buchwald S L．Palladiumcatalyzed intramolecular CO bond formation．JAm Chem Soc,2001,123(49):1220212206．[9] Vorogushin AV,Huang X,Buchwald S of tunable ligands allows for intermolecular Pdcatalyzed CO bond Am Chem Soc,2005,127(22)：81468149．[10] Mann G, Incarvito C,Rheingold A L,et CO coupling involving unactivated aryl halides．sterically induced reductive elimination to form the CO bond in diaryl Am Chem Soc,1999,121(13):32243225．[11] Shelby Q，Kataoka N，Mann G,et in situ ligand modification to generate a catalyst for room temperature aromatic CO bond Am Chem Soc,2000,122(43):1071810719．[12] Gao GY,Colvin A J,Chen Y,et synthesis of mesoaryloxyand alkoxysubstituted porphyrins via palladiumcatalyzed CO crosscoupling ,2003,5(18):32613264．[13] Harkal S,Kumax K,Michalik D,et al．An efficient catalyst system for dimaryl ether synthesis from aryl Lett,2005,46(18):32373240．[14]Sax K J,Saari W S,Maheney C L,et and infrared absorption spectra of phenyl Org Chem,1960,25:15905．[15]Xu LW,Xia GG,Li JW,et efficient CO crosscoupling reactions with inactivated halides by ligandless，heterogeneous raney NiAI alloy/copper(I) ,2003,(13):207l2073．[16] Lohmann S, Andrews S P,Burke B J,et palladiumcontaining perovskites：Catalysts for the Ullmann and Sonogashira ,2005,(8)：12911295．[17]Xing X,Padmanaban D,Yeh LA, et of a coppercatalyzed diaryl ether synthesis for thpreparation of ,2002,58(39)：79037910.[18]Smith K，Jones D，A superior synthesis of diaryl ethers by the use of ultrasound in the Ullmann them Soc,Perkin Trans l：Org BioOrg Chem(19721999),1992，(4)：407408．[19]Kumar S,Kapoor M,Surolia N,et al. Onestep synthesis of novel antimicrobial 2hydxoxy diaryl ethers through domestic microwave heating．Synth Commun，2004,34(3):413420．[20]Ma D,Cai ,Ndimethyl glycinepromoted Ullmann coupling reaction of phenols and aryl Lett,2003,5(21):37993802.[21]梅光軍，師偉，解科峰，[J].資源環(huán)境與工程，2007，21（3）:335338[22]Ma,.。Cai,Q.。Zhang,5,2453.[23]Zhang,H.。Cai,Q.。Ma,70,6154.[24]Kwong,.。Klapars,A.。Buchwald,4,581.[25]Kwong,.。Buchwald,5,793.[26](a)Lu,.。Twieg,.。Huang, 2003,44,6289.(b)Lu,.。Twieg, ,46,2997..二是帶頭接受監(jiān)督。要如履薄冰，嚴(yán)于自律，自覺接受黨和人民群眾的監(jiān)督。無論什么情況下，都要把握自己，潔身自好，清廉自守。要正確對待接受黨組織和職工群眾的監(jiān)督，勇于接受職工群眾的監(jiān)督。黨組織和職工群眾的監(jiān)督是一種警戒，是一面鏡子，經(jīng)常想一想，照一照，檢查一下自己有什么不足和缺點，及時加以改進和糾正，對自己的成長有好處。小洞不補，大洞吃苦。越是職位高權(quán)力大的干部，越要自覺監(jiān)督，任何人都沒有不受監(jiān)督的特權(quán)。要進一步拓寬民主監(jiān)督渠道，充分發(fā)揮各種監(jiān)督的作用。四是帶頭警示行為。黨中央向全黨敲響了警鐘，表明了我們黨同腐敗現(xiàn)象作斗爭的堅定決心。我本人作為一名基層人員，通過學(xué)習(xí)，思想覺悟有了進一步提高，認(rèn)真執(zhí)行黨的路線、方針、政策，決不能有任何偏離。
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