【正文】 目的：確保該設(shè)備的安裝符合國(guó)家壓力容器安裝要求 合格標(biāo)準(zhǔn)：《壓力容器安全技術(shù)監(jiān)察規(guī)定》 驗(yàn)證程序：檢查相關(guān)文件，核對(duì)現(xiàn)場(chǎng) 檢查結(jié)果：內(nèi)容設(shè)計(jì)要求現(xiàn)場(chǎng)檢查及結(jié)論備注材質(zhì)20g管板安全閥 Mpa壓力容器檢測(cè)報(bào)告壓力容器產(chǎn)品安全質(zhì)量檢驗(yàn)證書(shū)力學(xué)檢驗(yàn)報(bào)告焊縫射線檢測(cè)報(bào)告壓力試驗(yàn)檢驗(yàn)報(bào)告結(jié)論：執(zhí)行人： 日期： 復(fù)核人： 日期： 目的：保證在正常工作時(shí)，設(shè)備不會(huì)出現(xiàn)漏電現(xiàn)象。④ 保護(hù)接地電路的連接點(diǎn)牢固，沒(méi)有意外松脫的危險(xiǎn)。調(diào)試過(guò)程中進(jìn)行測(cè)試。2. 規(guī)格（是否符合材料配置要求）3. 管路走向（檢測(cè)其是否符合施工圖紙要求）制冷管路（檢測(cè)時(shí)依據(jù)供貨單位提供的質(zhì)量保證書(shū)）。1℃。3℃驗(yàn)證程序：——將溫度檢測(cè)儀測(cè)溫電阻通過(guò)驗(yàn)證接口放入樣品室內(nèi)。合格標(biāo)準(zhǔn)：從室溫（20℃）降至40℃的時(shí)間不大于60min。合格標(biāo)準(zhǔn)：1℃/min驗(yàn)證程序：按照凍干機(jī)使用標(biāo)準(zhǔn)操作規(guī)程操作，當(dāng)板層加熱開(kāi)始時(shí)記下當(dāng)時(shí)的溫度和時(shí)間，當(dāng)溫度升至50℃時(shí)，記下時(shí)間。驗(yàn)證程序：按照凍干機(jī)使用標(biāo)準(zhǔn)操作規(guī)程操作，當(dāng)冷凝器制冷開(kāi)始時(shí)記下當(dāng)時(shí)的溫度和時(shí)間，當(dāng)溫度降至40℃時(shí)，記下時(shí)間。 驗(yàn)證程序：——冷凝器制冷到50℃；——凍干箱加熱至35℃；——開(kāi)啟真空泵/真空泵組，記錄開(kāi)啟時(shí)間。合格標(biāo)準(zhǔn)：真空泄漏率為≤?m3/s 驗(yàn)證程序：——按照凍干機(jī)使用標(biāo)準(zhǔn)操作規(guī)程在空載狀態(tài)下運(yùn)行凍干機(jī)；——冷凝器制冷到50℃；——凍干箱加熱至35℃；——開(kāi)啟真空泵； ——當(dāng)達(dá)到極限真空度時(shí)，關(guān)閉真空大蝶閥保壓；——到達(dá)5Pa時(shí)開(kāi)始計(jì)時(shí)，觀察真空度變化。連續(xù)干燥24小時(shí)，停機(jī)稱(chēng)量平底托盤(pán)中的殘留注射用水的量，按照下列公式計(jì)算凍干機(jī)的最大捕水量。 真空保護(hù)：真空度設(shè)定為10~30Pa（可自己設(shè)定）,當(dāng)真空度超出此范圍時(shí)將報(bào)警。檢測(cè)項(xiàng)目及結(jié)果：按鈕狀態(tài)實(shí)驗(yàn)次數(shù)結(jié)論備注開(kāi)關(guān)壓縮機(jī)1壓縮機(jī)2板冷閥1板冷閥2摻冷閥冷凝器閥1冷凝器閥2循環(huán)泵1循環(huán)泵2真空泵1真空泵2水環(huán)泵大蝶閥小蝶閥摻氣閥前箱進(jìn)氣閥后箱進(jìn)氣閥液壓泵板層上升板層下降溢流閥前箱進(jìn)水閥后箱進(jìn)水閥前箱出水閥后箱出水閥電加熱有限量泄漏(啟動(dòng))真空?qǐng)?bào)警消警操作記錄冷凍干燥在位清洗在位消毒趨勢(shì)曲線工藝報(bào)表報(bào)警項(xiàng)目有效性結(jié)論備注有效無(wú)效水壓力空氣壓力真空?qǐng)?bào)警高壓報(bào)警1高壓報(bào)警2油壓差1油壓差2熱保護(hù)1熱保護(hù)2收液1收液2超溫報(bào)警`結(jié)論：執(zhí)行人： 日期： 復(fù)核人： 日期： 壓縮機(jī)組測(cè)試 目的：確認(rèn)壓縮機(jī)組的各項(xiàng)性能符合設(shè)計(jì)要求 合格標(biāo)準(zhǔn)及驗(yàn)證程序：依下列所示進(jìn)行開(kāi)機(jī)運(yùn)行，觀察各相關(guān)參數(shù)的具體數(shù)值，并進(jìn)行判斷檢測(cè)或檢查項(xiàng)目合格標(biāo)準(zhǔn)實(shí)測(cè)結(jié)果結(jié)論水循環(huán)系統(tǒng)冷卻水泵，冷凍水泵，冷卻塔風(fēng)機(jī)運(yùn)轉(zhuǎn)正常，水管及接口處不滲漏機(jī)組氣密性增壓試驗(yàn)充氮?dú)庵林评涔苈分校婵赵囼?yàn)關(guān)閉制冷機(jī)通大氣閥門(mén)，開(kāi)啟真空泵，停真空泵24H后，真空度下降不小于25 pa安全聯(lián)鎖系統(tǒng)冷卻水和冷凍水的壓力低于規(guī)定值時(shí)能進(jìn)行報(bào)警并停止工作數(shù)據(jù)記錄：檢測(cè)方法檢測(cè)數(shù)據(jù)結(jié)論時(shí)間壓力讀數(shù)漏點(diǎn)增壓試驗(yàn)真空試驗(yàn)檢查結(jié)果：結(jié)論：執(zhí)行人： 日期： 復(fù)核人： 日期： （模擬試生產(chǎn)） 目的：以模擬在正常生產(chǎn)情況下，凍干機(jī)能滿足凍干粉工藝要求 合格標(biāo)準(zhǔn)：產(chǎn)品質(zhì)量符合國(guó)家藥品標(biāo)準(zhǔn)WS1－（X－064）－2001Z 驗(yàn)證程序：依凍干機(jī)操作SOP，和產(chǎn)品的凍干工藝要求執(zhí)行，記錄下運(yùn)行時(shí)的相關(guān)參數(shù)，并對(duì)凍干后粉針進(jìn)行全檢，共做三批。 the second part is the interpretation of the two fundamental principles of the revision of laws and regulations in the party。s leadership, to solve the masses of the people reflect a focus on the problem. The new revision of the code and rule , reflects the party39。 the third is banned terms and discipline law, both with the party discipline, disciplinary regulations repeat and Criminal law and other laws and regulations repeat。s eighteen, ten eight plenary, the spirit of the Fourth Plenary Session of the Eleventh Central Committee and General Secretary Xi Jinping important instructions on the revised low political criterion and Regulations , highlighting the ruling party characteristics, serious discipline, the discipline quite in front of the law, based on the current, a longterm, advance as a whole, with Bu Xiuding independent rule and rule . Main principle is: first, adhere to the party constitution to follow. The constitution about discipline and selfdiscipline required specific, awaken the party constitution of party passes party consciousness, maintaining the authority of the constitution. General Secretary Xi Jinping pointed out that no rules, no side round. Party constitution is the fundamental law, the party must follow the general rules. In early 2015 held the eighth session of the Central Commission for Discipline Inspection Fifth Plenary Session of the 16th Central Committee, Xi Jinping again pointed out that constitution is the party must follow the general rules, but also the general rules. the revision of the code and rule is Method in adhere to the regulations established for the purpose of bining rule of virtue is to adhere to the party constitution as a fundamental to follow, the constitution authority set up, wake up the party constitution and party rules the sense of discipline, the party constitution about discipline and selfdiscipline specific requirements. 4 second is to adhere to in accordance with the regulations governing the party and the party. The Party of rule of virtue de, mainly refers to the party39。s advanced nature and purity, to reflect the revised standards requirements. Members of selfdiscipline norms around the party members how to correctly treat and deal with the public and private, cheap and rot thrifty and extravagance bitter music, put forward the four norms. Party leader cadre clean fingered selfdiscipline norms for the leadership of the party members and cadres of the vital few, around the clean politics, from civil servant of the color, the exercise of power, moral integrity, a good family tradition and other aspects of the leadership of the party members and cadres of the four norms norm norm. The Party member39。s leadership and the party39。s eighteen years implement the spirit of the central provisions of the eight, against the requirements of the four winds and transformation for disciplinary provisions, reflecting the style construction is always on the road, not a gust of wind. In the fight against corruption out of new problems, increase the trading rights, the use of authority relatives profit and other disciplinary terms. Prominent discipline of the masses, the new against the interests of the masses and ignore the demands of the masses and other disciplinary terms and make provisions of the disposition and the destruction of the party3