種蔬菜基質(zhì)中不同技術(shù)分析農(nóng)藥殘留(參考版)
2025-01-07 15:21本頁(yè)面
【正文】 乙酰甲胺磷 氧化樂(lè)果 樂(lè)果 甲基對(duì)硫磷 不同蔬菜樣品在 MRM模式下分析得到的總離子流圖 甘藍(lán) 芹菜 甘藍(lán) 芹菜 普通白菜 豇豆 不同蔬菜樣品在 MRM模式下分析得到的總離子流圖 韭菜 不同蔬菜樣品在 MRM模式下分析得到的總離子流圖 由于 GCQ 能夠?qū)⒋蟛糠謽悠坊|(zhì)干擾“過(guò)濾”掉，所以即使基質(zhì)干擾相對(duì)比較大的韭菜樣品 ,其 TIC圖與其它品種蔬菜的結(jié)果相比也沒(méi)有明顯區(qū)別 甘藍(lán)樣品 23種農(nóng)藥 MRM分析結(jié)果 芹菜樣品 23種農(nóng)藥 MRM分析結(jié)果 普通白菜樣品 23種農(nóng)藥 MRM分析結(jié)果 Page 58 豇豆樣品 23種農(nóng)藥 MRM分析結(jié)果 (不知何故豇豆當(dāng)中所有農(nóng)藥的響應(yīng)值都很低） Page 59 韭菜樣品 23種農(nóng)藥 MRM分析結(jié)果 甘藍(lán) Compound RT Final Conc (純?nèi)軇?biāo)曲） Final Conc (對(duì)照標(biāo)曲） 1 敵敵畏 ng/ml ng/ml 2 甲胺磷 ng/ml ng/ml 3 乙酰甲胺磷 ng/ml ng/ml 4 氧樂(lè)果 ng/ml ng/ml 5 甲拌磷 ng/ml ng/ml 6 二嗪磷 ng/ml ng/ml 7 嘧霉胺 ng/ml ng/ml 8 樂(lè)果 ng/ml ng/ml 9 甲基對(duì)硫磷 ng/ml ng/ml 10 馬拉硫磷 ng/ml ng/ml 11 毒死蜱 ng/ml ng/ml 12 三唑酮 ng/ml ng/ml 13 對(duì)硫磷 ng/ml ng/ml 14 氟蟲(chóng)腈 ng/ml ng/ml 15 甲基異柳磷 ng/ml ng/ml 16 水胺硫磷 ng/ml ng/ml 17 丙溴磷 ng/ml ng/ml 18 三唑磷 ng/ml ng/ml 19 甲氰菊酯 ng/ml ng/ml 20 亞安硫磷 ng/ml ng/ml 21 伏殺硫磷 ng/ml ng/ml 22 噠螨靈 ng/ml ng/ml 23 苯嘧甲環(huán)唑 ng/ml ng/ml 芹菜 Compound RT Final Conc (純?nèi)軇?biāo)曲） Final Conc (對(duì)照標(biāo)曲） 敵敵畏 ng/ml ng/ml 甲胺磷 ng/ml ng/ml 乙酰甲胺磷 ng/ml ng/ml 氧樂(lè)果 ng/ml ng/ml 甲拌磷 ng/ml ng/ml 二嗪磷 ng/ml ng/ml 嘧霉胺 ng/ml ng/ml 樂(lè)果 ng/ml ng/ml 甲基對(duì)硫磷 ng/ml ng/ml 馬拉硫磷 ng/ml ng/ml 毒死蜱 ng/ml ng/ml 三唑酮 ng/ml ng/ml 對(duì)硫磷 ng/ml ng/ml 氟蟲(chóng)腈 ng/ml ng/ml 甲基異柳磷 ng/ml ng/ml 水胺硫磷 ng/ml ng/ml 丙溴磷 ng/ml ng/ml 三唑磷 ng/ml ng/ml 甲氰菊酯 ng/ml ng/ml 亞安硫磷 ng/ml ng/ml 伏殺硫磷 ng/ml ng/ml 噠螨靈 ng/ml ng/ml 苯嘧甲環(huán)唑 ng/ml ng/ml 普白 Compound RT Final Conc (純?nèi)軇?biāo)曲） Final Conc (對(duì)照標(biāo)曲） 1 敵敵畏 ng/ml ng/ml 2 甲胺磷 ng/ml ng/ml 3 乙酰甲胺磷 ng/ml ng/ml 4 氧樂(lè)果 ng/ml ng/ml 5 甲拌磷 ng/ml ng/ml 6 二嗪磷 ng/ml ng/ml 7 嘧霉胺 ng/ml ng/ml 8 樂(lè)果 ng/ml ng/ml 9 甲基對(duì)硫磷 ng/ml ng/ml 10 馬拉硫磷 ng/ml ng/ml 11 毒死蜱 ng/ml ng/ml 12 三唑酮 ng/ml ng/ml 13 對(duì)硫磷 ng/ml ng/ml 14 氟蟲(chóng)腈 ng/ml ng/ml 15 甲基異柳磷 ng/ml ng/ml 16 水胺硫磷 ng/ml ng/ml 17 丙溴磷 ng/ml ng/ml 18 三唑磷 ng/ml ng/ml 19 甲氰菊酯 ng/ml ng/ml 20 亞安硫磷 ng/ml ng/ml 21 伏殺硫磷 ng/ml ng/ml 22 噠螨靈 ng/ml ng/ml 23 苯嘧甲環(huán)唑 ng/ml ng/ml 韭菜 Compound RT Final Conc (純?nèi)軇?biāo)曲） Final Conc (對(duì)照標(biāo)曲） 1 敵敵畏 ng/ml ng/ml 2 甲胺磷 ng/ml ng/ml 3 乙酰甲胺磷 ng/ml ng/ml 4 氧樂(lè)果 ng/ml ng/ml 5 甲拌磷 ng/ml ng/ml 6 二嗪磷 ng/ml ng/ml 7 嘧霉胺 ng/ml ng/ml 8 樂(lè)果 ng/ml ng/ml 9 甲基對(duì)硫磷 ng/ml ng/ml 10 馬拉硫磷 ng/ml ng/ml 11 毒死蜱 ng/ml ng/ml 12 三唑酮 ng/ml ng/ml 13 對(duì)硫磷 ng/ml ng/ml 14 氟蟲(chóng)腈 ng/ml ng/ml 15 甲基異柳磷 ng/ml ng/ml 16 水胺硫磷 ng/ml ng/ml 17 丙溴磷 ng/ml ng/ml 18 三唑磷 ng/ml ng/ml 19 甲氰菊酯 ng/ml ng/ml 20 亞安硫磷 ng/ml ng/ml 21 伏殺硫磷 ng/ml ng/ml 22 噠螨靈 ng/ml ng/ml 23 苯嘧甲環(huán)唑 ng/ml ng/ml 豇 豆？？？ Compound RT Final Conc (純?nèi)軇?biāo)曲） Final Conc (對(duì)照標(biāo)曲） 敵敵畏 ng/ml ng/ml 甲胺磷 ng/ml ng/ml 乙酰甲胺磷 ng/ml ng/ml 氧樂(lè)果 ng/ml ng/ml 甲拌磷 ng/ml ng/ml 二嗪磷 ng/ml ng/ml 嘧霉胺 ng/ml ng/ml 樂(lè)果 ng/ml ng/ml 甲基對(duì)硫磷 ng/ml ng/ml 馬拉硫磷 ng/ml ng/ml 毒死蜱 ng/ml ng/ml 三唑酮 ng/ml ng/ml 對(duì)硫磷 ng/ml ng/ml 氟蟲(chóng)腈 ng/ml ng/ml 甲基異柳磷 ng/ml ng/ml 水胺硫磷 ng/ml ng/ml 丙溴磷 ng/ml ng/ml 三唑磷 ng/ml ng/ml 甲氰菊酯 ng/ml ng/ml 亞安硫磷 ng/ml ng/ml 伏殺硫磷 ng/ml ng/ml 噠螨靈 ng/ml ng/ml 苯嘧甲環(huán)唑 ng/ml ng/ml 。 1 2 . 4 5 1 2 . 5 0 1 2 . 5 5 1 2 . 6 0 1 2 . 6 5 1 2 . 7 0 1 2 . 7 5 1 2 . 8 0 1 2 . 8 5 1 2 . 9 002022400060008000100001202214000160001800020220220222400026000280003000032022T i m e A b u n d a n c eI o n 9 3
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