【正文】 ...... 8 工藝流程框圖 ................................................................................................... 9 肟鹽處理反應(yīng)工段工藝流程框圖 ............................................................ 9 5181 反應(yīng)工段和后處理工段反應(yīng)流程圖 ............................................ 10 第 3 章 物料衡算 ...................................................................................................11 概述 ..................................................................................................................11 物料衡算的原理 ..............................................................................................11 物料衡算的基準(zhǔn)與任務(wù) ..................................................................................11 衡算基準(zhǔn) ...................................................................................................11 設(shè)計(jì)任務(wù) ...................................................................................................11 各步驟收率 ......................................................................................................11 各反應(yīng)單元 ..................................................................................................... 12 江西科技師范大學(xué)本科畢業(yè)論文 II 游離反應(yīng) .................................................................................................. 12 萃取洗滌 .................................................................................................. 14 冷卻濃縮 .................................................................................................. 15 醚化和 硅烷化 .......................................................................................... 16 分層萃取 .................................................................................................. 18 濃縮與頂蒸 .............................................................................................. 20 離心工段 .................................................................................................. 21 干燥 .......................................................................................................... 23 第 4 章 熱量衡算 .................................................................................................. 24 熱量衡算依據(jù) ................................................................................................. 24 設(shè)備的熱量平衡方程式 .......................................................................... 24 熱量衡算基礎(chǔ)數(shù)據(jù)的計(jì)算和查取 .......................................................... 24 總體能量衡算 ................................................................................................. 25 能量衡算目的 ................................................................................................. 25 干燥工序的熱量衡算 ..................................................................................... 25 第 5 章 設(shè)備選型和計(jì)算 ...................................................................................... 27 工藝設(shè)備選型概述 ......................................................................................... 27 GMP 對設(shè)備選型和安裝的要求 .................................................................... 27 計(jì)算依據(jù) ......................................................................................................... 27 主要反應(yīng)設(shè)備選型 ......................................................................................... 28 反應(yīng)釜 ...................................................................................................... 28 計(jì)量罐 ...................................................................................................... 31 儲(chǔ)罐 .......................................................................................................... 33 高效過濾器 .............................................................................................. 34 冷凝器 ...................................................................................................... 35 離心泵 ...................................................................................................... 35 廢液貯池 .................................................................................................. 36 第 6 章 車間布置設(shè)計(jì) .......................................................................................... 37 江西科技師范大學(xué)本科畢業(yè)論文 III 工廠設(shè)計(jì)的內(nèi)容與規(guī)范 ................................................................................. 37 車間概況 ......................................................................................................... 37 車間形式 .................................................................................................. 38 廠房的層數(shù) .............................................................................................. 38 廠房平面布置 .......................................................................................... 38 設(shè)備布置的基本要求 ..................................................................................... 39 設(shè)備排列順序 .......................................................................................... 39 設(shè)備排列方法 .......................................................................................... 39 操作間距 .................................................................................................. 39 第 7 章 “三廢”處理及綜合利用 ........................................................................ 40 “三廢”排放情況 ......................................................................................... 40 廢水處理 .................................................................................................. 40 廢氣處理 .................................................................................................. 40 廢渣處理 .................................................................................................. 41 噪聲污染情況及處理 ..................................................................................... 41 套用與回收利用 ............................................................................................. 41 第 8 章 勞動(dòng)組織與崗位定員 ...........