【正文】 .................. .................72 色譜柱安裝 ............................ .......................................................................73 1061進(jìn)樣器操作 .......................... ..................................................................76 1061進(jìn)樣器測(cè)試 ................................................ .......... .................................78 閥控系統(tǒng) ......................................................................................... .................................80 檢測(cè)器 .............................................................................................................................84 介紹 ...........................................................................................................................84 火焰離子光度檢測(cè)器（ FID） ........................................................................................85 初始設(shè)定 ........................................................................................................85 操作 ..............................................................................................................86 檢測(cè)器程序 ...................................... .......... ...................................................86 安裝 /拆卸 ..............................................................................................88 氮 /磷檢測(cè)器（ TSD） ...............................................................................................93 初始設(shè)定 .........................................................................................................93 操作及推薦條件 ........................................ ........... ........... .....................94 TSD裝配圖 ..................................... ........................................ ....................100 熱導(dǎo)檢測(cè)器 (TCD)............................................................................. .........................105 初始設(shè)定 ................................................................................................105 操作 ............................................................................... ........... ................107 調(diào)節(jié) TCD載氣流量 ....................................... ........... ...................................113 電子捕獲檢測(cè)器 (ECD)...................... ..............................................................................115 初始設(shè)定 .......................................................................................................115 ECD氣路 ................... .................................................... .............................120 安裝 /拆卸 ............................................................. ........... ........... ................121 脈沖火焰光度檢測(cè)器 (PFPD) ..................................................................................125 通訊 ................................................................. .................................................126 介紹 .........................................................................................................................126 以太網(wǎng) (Ether )通訊 ..................................................................................................126 模擬信號(hào)通訊 ....................................................................................................131 本地自動(dòng)化 .................................................................................................................134 介紹 ............................ ........... ....... .......... .... ............... .......... .......... ..........................134 不可尋址的自動(dòng)化 ........................... ......... ......... ........................................................135 可尋址自動(dòng)化 ................................... ......... ..............................................................135 自動(dòng)化控制 ................................................ ......... ....................................................... 135 自動(dòng)化方法 ............................................... ......... ....................................................137 單一方法，不可尋址自動(dòng)化 ........................ ........ .......... ........... ....................................138 方法序列，不可尋址自動(dòng)化 ........................ ......... ...................... ........... .......................138 單一方法，可尋址自動(dòng)化 ............................ ......... ........... ........ ....................................140 方法序列，不可尋址自動(dòng)化 ... ......... ........... ........... ........... ....................... ...................141 8200自動(dòng)進(jìn)樣器控制 ................................... ......... ............................... .........................141 自動(dòng)化狀態(tài) .............................................................................................................. 142 可尋址自動(dòng)化狀態(tài)屏幕 (8200 自動(dòng)化 )........... ........ .................... ........... .......................143 不可尋址自動(dòng)化狀態(tài)屏幕 .................................................. ........ ........... ........... ..........143 插圖 Figure 1 1079進(jìn)樣器裝配圖 .............................................................................................44 Figure 2進(jìn)樣器氣體流程圖 .............................................................................................48 Figure 3 電子流量控制器（ EFC）圖示 ............................................................................49 Figure 4 1079進(jìn)樣器毛細(xì)柱安裝 ........................ ............................................................50 Figure 5 1041 通用進(jìn)樣器配備內(nèi)襯 ............................................. ....................................65 Figure 6 毛細(xì)柱尾端 .........................................................................................................66 Figure 7 1061閃蒸進(jìn)樣器配備內(nèi)襯 ....................................... .......... ..............................73 Figure 8 毛細(xì)柱端頭 ............................................................................................ ............75 Figure 9 FID 分解圖 ................................................................................... ...