【正文】
EDTA plexometric titration, if necessary, used atomic absorption to verification, in particular the appearance of suspicious samples, which to antiadulteration. ? 重金屬 Heavy metals:鉻 Cr、鉛 Pb、鎘 Cd 28 謝謝觀看 /歡迎下載 BY FAITH I MEAN A VISION OF GOOD ONE CHERISHES AND THE ENTHUSIASM THAT PUSHES ONE TO SEEK ITS FULFILLMENT REGARDLESS OF OBSTACLES. BY FAITH I BY FAITH 。 游離水 %= 100 m2m1 m The determination method of free water in CuSO4?5H2O 27 MnSO4恒重的 G4玻芯坩堝內(nèi) ,用無水丙酮在抽濾下洗 56次 ,然后在 50 C176。5H2O的質(zhì)控要點: Quality control of Copper Sulfate ? 含量 Content ? 防結(jié)塊劑(載體)的種類 硬脂酸鈣、白炭黑、石粉 The types of antiblocking agent (carrier) calcium stearate, silica aerogel, mountain flour ? 砷 As、鉛 Pb、鎘 Cd、鉻 Cr。同時做空白。 Determination method of oxidation substances residual in Zinc Sulfate 23 FeSO4 Determination method of Zinc Sulfate content 22 硫酸鋅氧化劑殘留的測定方法 ? 定性的方法:按配方制備 500克,混勻后裝入樣品袋,放入 40℃ 的培養(yǎng)箱內(nèi)保溫 35天,觀察顏色變化。移取此溶液 250ml三角瓶內(nèi)再加 30ml水,加甲基紅 (2g/L)3滴 ,加氨水 (1+1) 至溶液呈黃色 ,有棕紅色沉淀 ,并略帶氨味,沸水浴煮沸 3min,趁熱過濾(定量濾紙),并用 NH4NO3(10g/L)洗滌 56次 ,濾液全部收于 250ml三角瓶內(nèi) ,向濾液中滴加 HCl (1+1)到剛有沉淀生成,加 25mlNH3NH4Cl緩沖液( PH=10),加鉻黑 T指示劑少許,用 EDTA標(biāo)準(zhǔn)溶液 [cEDTA) =(或 )mol/l]滴定到溶液呈純藍色。 同時做空白試驗。 Concern about the stability of Ferrous Sulfate. 19 三、銅鐵鋅錳微量元素添加劑質(zhì)控要點 ZnSO4 Abovementioned two major factors, the residual of oxidation substances in Zinc Sulfate is more important (crucial). So feedgrade Zinc Sulfate should put residual of oxidation substances as quality control item. Summary: Analysis of discoloration