【正文】 ............................................................3 原料路線的選擇..........................................................................................3 生產(chǎn)方法的可行..........................................................................................3 生產(chǎn)規(guī)模的確定..........................................................................................3第三章 產(chǎn)品方案..........................................................................................4 產(chǎn)品名稱與性質(zhì)..........................................................................................4 性狀及理化性質(zhì)..........................................................................................4 產(chǎn)品的質(zhì)量規(guī)格..........................................................................................4 產(chǎn)品的生產(chǎn)制度..........................................................................................4 包裝與儲(chǔ)藏.................................................................................................4第四章 生產(chǎn)方法與主要工藝流程..............................................................5 生產(chǎn)方法....................................................................................................5 主要流程....................................................................................................5第五章 生產(chǎn)工藝控制和中間體質(zhì)量標(biāo)準(zhǔn)..................................................6 生產(chǎn)工藝控制.............................................................................................6 中間體質(zhì)量標(biāo)準(zhǔn)..........................................................................................6第六章 物料衡算..........................................................................................7 配堿過程....................................................................................................7 反應(yīng)過程....................................................................................................8 甲醇回收過程.............................................................................................9第七章 能量衡算........................................................................................11 計(jì)算依據(jù)..................................................................................................11 計(jì)算過程..................................................................................................11 單耗表.....................................................................................................15第八章 工藝設(shè)備選型與設(shè)計(jì)計(jì)算............................................................17 設(shè)計(jì)方法與原則........................................................................................17 設(shè)計(jì)計(jì)算..................................................................................................17第九章 車間布置設(shè)計(jì)................................................................................21 車間劃分依據(jù)...........................................................................................21 車間的布置設(shè)計(jì)........................................................................................21 設(shè)備間的距離...........................................................................................21 安全和防腐要求........................................................................................21第十章 勞動(dòng)組織和安全生產(chǎn)....................................................................22 安全生產(chǎn)................................................................................................22第十一章 “三廢”及綜合處理...................................................................23 廢水的排放及處理...................................................................................23 廢渣的排放及處理...................................................................................23 廢氣的排放及處理...................................................................................24結(jié)束語..........................................................................................................25心得體會(huì)......................................................................................................26參考文獻(xiàn)......................................................................................................27附錄Ⅰ 設(shè)備一覽表....................................................................................28附錄Ⅱ 物料流程框圖................................................................................2929設(shè)計(jì)簡介對(duì)硝基苯甲醚又稱對(duì)硝基茴香醚(P—nitro anisole)，是染料的重要中間體對(duì)氨基苯甲醚的重要前期化合物．對(duì)硝基苯甲醚的產(chǎn)量與質(zhì)量直接影響著對(duì)氨基苯甲醚的產(chǎn)量與質(zhì)量，因此長期以來不少學(xué)者對(duì)其合成進(jìn)行了不少探討。本設(shè)計(jì)書根據(jù)設(shè)計(jì)要求和關(guān)鍵參數(shù)，設(shè)計(jì)了合理的工藝流程，繪制了工藝流程圖。設(shè)計(jì)重點(diǎn)主要在：全流程物料衡算，熱量衡算，設(shè)備設(shè)計(jì)與選型，流程設(shè)計(jì)及車間布置設(shè)計(jì)。四、參考文獻(xiàn)[1] ,1985.[2] ,1986.[3] ,1989.[4] .[5] 化工設(shè)備及機(jī)械產(chǎn)品樣本匯編.[6] ,1985.[7] 徐永文,化學(xué)工業(yè)出版社.[8] .[9] 催克清,張禮敬,[M].北京：化學(xué)工業(yè)出版社,2004．[10] 王紅林,2005．[11] [M].北京：化學(xué)工業(yè)出版社,2000.設(shè)計(jì)報(bào)告書摘要本設(shè)計(jì)書設(shè)計(jì)了以對(duì)硝基氯苯、甲醇和氫氧化鈉為原料，用芐基三乙基氯化銨作相轉(zhuǎn)移催化劑，在常壓下合成對(duì)硝基苯甲醚的工藝路線。3．第二周 繼續(xù)查閱資料；能量計(jì)算；結(jié)合工程設(shè)備選型；繪制工藝流程圖。三、時(shí)間安排1．設(shè)計(jì)時(shí)間為3周，即20108232010926。學(xué)習(xí)查閱主要的工藝設(shè)計(jì)數(shù)據(jù)參考書，正確地進(jìn)行工藝過程的物料衡算和熱量衡算并進(jìn)行設(shè)備的選型和設(shè)計(jì)計(jì)算。并用計(jì)算機(jī)畫出帶有工藝控制點(diǎn)的工藝流程圖。二、基本內(nèi)容和要求 學(xué)習(xí)工藝設(shè)計(jì)的基本原理、方法和應(yīng)遵循的原則。解決化工產(chǎn)品生產(chǎn)車間設(shè)計(jì)實(shí)際問題的能力，掌握化工工藝流程設(shè)計(jì)、物料恒算、設(shè)備選型、車間工藝布置設(shè)計(jì)等的基本方法和步驟；從技術(shù)上的可行性與合理性兩個(gè)方面樹立正確的設(shè)計(jì)思想。一、任務(wù)和目的對(duì)硝基苯甲醚是一種重要的中間體，主要用于生產(chǎn)染料、農(nóng)藥和醫(yī)藥工業(yè)中。對(duì)硝基苯甲醚的工藝設(shè)計(jì)的目的，主要是以專業(yè)基礎(chǔ)課的學(xué)習(xí)為基礎(chǔ)，針對(duì)要求的化工項(xiàng)目，設(shè)計(jì)合理的工藝流程，選擇相應(yīng)的工藝設(shè)備等。通過本課程設(shè)計(jì)，提高運(yùn)用計(jì)算機(jī)設(shè)計(jì)繪圖(AutoCAD)的能力。能依據(jù)給出的設(shè)計(jì)要求和關(guān)鍵參數(shù)，能設(shè)計(jì)提出合理的工藝流程。寫出工藝操作過程及過程分析、控制要點(diǎn)。完成設(shè)計(jì)說明書的編寫并提交打印件。2．第一周 進(jìn)行課程設(shè)計(jì)動(dòng)員、下達(dá)課程設(shè)計(jì)任務(wù)書；查閱資料、確定生產(chǎn)工