【正文】
想。其他實(shí)驗(yàn)參數(shù)如 注入 溫度和粒子濃度似乎沒有明顯影響 磷化銦 納米晶體大小或粒徑分布。 使用一個真正的連續(xù)三階段的微流控反應(yīng)堆來精確 協(xié)調(diào) 混合、老化和連續(xù)增長 狀態(tài) 的反應(yīng)條件 ,我們這里描述的研究建立在之前的銦 的納米晶體合成和機(jī)械的工作 之上 來探測 重要的 實(shí)驗(yàn)參數(shù) 包含 InP 納米晶體的合成。m 提供 所譯外文資料附件(印刷類含封面、封底、目錄、翻譯部分的復(fù)印件等,網(wǎng)站類的請附網(wǎng)址及原文 】 Investigation of Indium Phosphide Nanocrystal Synthesis Using a High Temperature and HighPressure Continuous Flow Microreactor Jinyoung Baek, Peter M. Allen, Moungi G. Bawendi,* and Klavs F. Jensen Indium phosphide (InP) nanocrystals[1]are of significant interest for use in optoelectronic devices, specifically as a replacement for CdSe nanocrystals in mercial applications. However, the current mechanistic understanding and synthetic procedures for InP nanocrystals has not yet reached the same level as for CdSe nanocrystal synthesis.[2] Using a truly continuous threestage microfluidic reactor to precisely tune reaction conditions in the mixing, aging, and sequential growth regimes, our study described here builds on previous InP nanocrystal synthetic[3] and mechanistic work[4] to probe the significant experimental parameters involved in InP nanocrystal syntheses. We find that the growth of InP nanocrystals is dominated by the aging regime, which is consistent with a model of InP nanocrystal growth where nanocr