【正文】 甲基丙烯酸二甲氨基乙酯的合成 The synthesis of dimethyl amino ethyl methacrylate 目錄 摘要 ................................................................................................................................................. I Abstract .........................................................................................................................................II 引言 ................................................................................................................................................ 1 第 一 章 綜述 ............................................................................................................................... 2 甲基丙烯酸二甲氨基乙酯的性質(zhì)用途 ............................................................................ 2 物化性質(zhì) ........................................................................................................................ 2 用途 ................................................................................................................................ 2 甲基丙烯酸二甲氨基乙酯的合成方法研究 .................................................................... 5 醇酸直接酯化法 ............................................................................................................ 5 酰氯酯化法 .................................................................................................................... 5 酯交換法 ........................................................................................................................ 5 DMEAMA 的開(kāi)發(fā)前景 ..................................................................................................... 6 研究的內(nèi)容 ........................................................................................................................ 7 第 二 章 實(shí)驗(yàn)部分 ...................................................................................................................... 8 實(shí)驗(yàn)試劑 ........................................................................................................................... 8 實(shí)驗(yàn)儀器 ........................................................................................................................... 8 實(shí)驗(yàn)步驟 ........................................................................................................................... 8 正交實(shí)驗(yàn)方案設(shè)計(jì) ............................................................................................................ 9 紅外光譜概述 ..................................................................................................................10 紅外光譜劃分 ...............................................................................................................10 紅外光譜圖 ...................................................................................................................10 紅外光譜儀基本工作原理 ........................................................................................... 11 紅外光譜圖的三要素 ................................................................................................... 11 有機(jī)化合物結(jié)構(gòu)分析 ...................................................................................................12 主要應(yīng)用 ........................................................................................................................12 第 三 章 結(jié)果與分析 ................................................................................................................13 IR 譜圖分析 ......................................................................................................................13 實(shí)驗(yàn)結(jié)果分析 ..................................................................................................................13 催化劑用量對(duì) DMEAMA 的影響 ...............................................................................13 原料配比對(duì) DMAEMA 的影響 ...................................................................................14 反應(yīng)時(shí)間對(duì) DMAEMA 的影響 ...................................................................................15 結(jié)論 ...............................................................................................................................................17 致謝 .................................................................................................................... 錯(cuò)誤 !未定義書(shū)簽。 參考文獻(xiàn) .....................................................................................................................................19 I 甲基丙烯酸二甲氨基乙酯的合成 摘要 ： 本課題研究的是甲基丙烯酸二甲氨基乙酯 (DMEAMA)的合成，甲基丙烯酸二甲氨基乙酯 (DMEAMA)是一種多功能的活性單體，具有烯烴、胺、酯類化合物的特