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基矢長度,以兩端為圓心分別 a,端點(diǎn)的連線 距離為 t,如果這兩個端點(diǎn)也是陣點(diǎn),其連線必為 基矢 t0的整數(shù)倍,即 t=mt0=2t0cosa+t0, 解出 a=?, 2/3?, ?/2 ?/3, 0,對應(yīng) 2, 3, 4, 6次軸和沒有旋轉(zhuǎn)。 Al2O3中氧原子的觀察 HAADF and ABF images of αAl2O3 (bulk) viewed along the [1210] zone axis. The Known structure is indicated, and simulated data is overlaid on the experimental images. . Findlay, et al., Ultramicroscopy V111(2023), 285289 Direct imaging of hydrogenatom columns in a crystal by annular brightfield electron microscopy Ryo Ishikawa, et al., NATURE MATERIALS V 10 (2023), 278281 YH2的原子模型 (a), ABF(b), ADF(c), HAADF(d) C. Colliex, lecture 2 4D (x,y,E,t) Spectrumimaging mode + HAADF signal e e e e e e e e e e e e e e Sample at each pixel ? 50 spectra/pixel ? 3 ms/spectrum ? deconvolution Improved energy resolution ( eV) STEM+EELS Kimoto, K., et al., Nature, 2023. 450(7170): p. 702704. Botton, ., S. Lazar, and C. Dwyer,. Ultramicroscopy, 2023. 110(8): p. 926934. . Corrected 80 kV STO/BTO Ba Sr Ti La N4,5 La M4,5 Ti O K Mn L2,3 La N4,5 La M4,5 SrTiO3 [100] EELS mapping at 200kV (STEM) STEM (DF) 96x73 pixels 150pA probe current Sr Ti O Sr Ti Sr O Ti O STEM+EDS Chu, ., et al., Physical Review Letters, 2023. 104(19): p. 196101. D39。C 130186。 nbg ????如果我們能在離焦會聚束電子衍射圖中,找到 3條都穿過位錯線,但不屬于同一個 Laue帶的衍射線,則可根據(jù)衍射線與位錯線相互作用的分裂情況,列出三個線性無關(guān)的方程, 解這個方程組即可確定位錯的 Burgers矢量。 (a) (b) CBED應(yīng)變模擬 : Direct observation of dorbital holes and Cu–Cu bonding in Cu2O J. M. Zuo et al, Nature (1999), 401, 49–52 定量會聚束電子衍射 掃描透射電子顯微學(xué) scanning transmission electron microscopy (STEM) 電子槍 會聚鏡 束偏轉(zhuǎn)器 物鏡 樣品 掃描電鏡( SEM) 掃描發(fā)生器 探測器 顯示器 TEM vs STEM TEM與 STEM:倒易原理 Liu, J. (2023). Scanning transmission electron microscopy of nanoparticles. In Characterization of